中国农业科学 ›› 2021, Vol. 54 ›› Issue (8): 1772-1786.doi: 10.3864/j.issn.0578-1752.2021.08.016
收稿日期:
2020-08-14
接受日期:
2021-01-25
出版日期:
2021-04-16
发布日期:
2021-04-25
作者简介:
张清安,Tel:13572932273;E-mail: 基金资助:
ZHANG QingAn1,2(),XU BoWen1,CHEN BoYu1,ZHANG BaoShan1,CHENG Shuang2
Received:
2020-08-14
Accepted:
2021-01-25
Online:
2021-04-16
Published:
2021-04-25
摘要:
【目的】明确超声降低高级醇对红酒风味所带来的影响,了解其风味形成机制,为超声技术应用于降低高级醇并促进红酒风味品质的改善提供理论依据。【方法】首先采用电子舌和电子鼻对不同超声条件处理后的红酒进行测定,并对所得结果用主成分分析(PCA)和判别函数分析(DFA)研究红酒风味品质的变化;随后用气质联用技术分析最优降低高级醇的超声参数处理后红酒中挥发性成分的变化;最后,以正丙醇、异戊醇、正戊醇和异丁醇标准品为添加物构建含高级醇的模型酒液体系,探究超声降解高级醇时对红葡萄酒风味变化的具体影响机制。【结果】单因素实验结果表明,超声处理条件对红酒感官品质的影响用电子鼻、电子舌判定差异不显著(尤其电子鼻的判定结果);气质联用分析表明,超声不仅能够增加酒中挥发性物质的种类,还可以显著增加酯类等物质的相对含量,同时降低酸类、醇类等的含量;模型酒液体系研究结果与上述变化情况基本一致。【结论】超声处理不仅可以有效降低红酒中高级醇的含量,还可以促进红酒中挥发性风味物质的形成,进而改善酒的风味品质,结果可为超声技术用于改善红酒品质提供一定的理论依据。
张清安,徐博文,陈博宇,张宝善,程爽. 超声降低红酒中高级醇含量对酒体风味特性的影响[J]. 中国农业科学, 2021, 54(8): 1772-1786.
ZHANG QingAn,XU BoWen,CHEN BoYu,ZHANG BaoShan,CHENG Shuang. Changes of Wine Flavor Properties from the Decreased Higher Alcohols Induced by Ultrasound Irradiation[J]. Scientia Agricultura Sinica, 2021, 54(8): 1772-1786.
表2
电子鼻性能描述"
传感器名称 Sensor name | 性能描述 Performance description |
---|---|
S1 | 氨气、胺类 Ammonia, amines |
S2 | 硫化氢、硫化物 Hydrogen sulfide, sulfide |
S3 | 氢气 Hydrogen |
S4 | 酒精、有机溶剂 Alcohol, organic solvent |
S5 | 醇类、酮类、醛类、芳香族化合物 Alcohols, ketones, aldehydes, aromatic compounds |
S6 | 甲烷、沼气、天然气 Methane, marsh gas, natural gas |
S7 | 可燃性气体 Combustible gas |
S8 | 挥发性有机物 Volatile organic compounds |
S9 | 液化气、天然气、煤气 Liquefied gas, natural gas, gas |
S10 | 液化气、可燃气体 Liquefied gas, combustible gas |
S11 | 烷烃、酒精、天然气、烟雾 Alkane, alcohol, natural gas, smoke |
S12 | 酒精、有机溶剂 Alcohol, organic solvent |
S13 | 烟气、烹调臭味 Smoke, cooking odor |
S14 | 甲烷、燃气 Methane, gas |
表4
超声处理前后红酒中香气物质的变化"
类别 Variety | 化合物 Compound | 相对百分含量Relative content (%) | |
---|---|---|---|
处理前Before | 处理后After | ||
酸类 Acids | L-乳酸 L-Lactic acid | 26.18 | 18.47 |
胞壁酸 Parietal acid | 0.24 | 0.25 | |
正癸酸 Decanoic acid | 0.76 | 0.82 | |
己酸 Caproic acid | 0.51 | - | |
二十二碳六烯酸 Docosahexaenoic acid | 0.04 | - | |
辛酸 Caprylic acid | 2.10 | - | |
壬酸 Nonylic acid | 0.21 | 0.26 | |
癸醛 Decyl aldehyde | - | 0.28 | |
油酸 Oleic acid | - | 0.19 | |
4-氨基-1,5-戊二酸 4-amino-1,5-glutaric acid | - | 0.22 | |
酯类 Esters | 2-羟基丙酸乙酯 Ethyl 2-hydroxypropionate | 17.57 | 28.25 |
乳酸异戊酯 Isoamyl lactate | 0.48 | 0.17 | |
己酸乙酯 Ethyl hexanoate | 1.76 | 1.23 | |
丁二酸二乙酯 Diethyl succinate | 7.26 | 8.37 | |
辛酸乙酯 Ethyl caprylate | 2.32 | 1.82 | |
异胆酸乙酯 Ethyl isocholate | 0.55 | 1.23 | |
十六烷酸乙酯 Ethyl hexadecane | 1.18 | 1.35 | |
十八酸乙酯 Ethyl octadecanoate | 0.48 | 0.31 | |
7-甲基-Z-四癸烯-1-醇乙酸酯 7-methyl-z-tetradecene-1-ol acetate | 0.25 | 0.61 | |
1,2-苯二甲酸正辛酯 1,2-noctyl-phthalate | 0.11 | 0.23 | |
癸酸乙酯 Ethyl decanoate | 0.21 | 0.25 | |
丁二酸3-甲基丁基酯 Succinic acid 3-methyl butyl ester | 0.37 | 0.37 | |
Z-(13,14-环氧)四聚-11-烯-1-醇乙酸酯 Z-(13,14-epoxy) tetra-11-ene-1-ol acetate | 0.12 | 0.27 | |
2-苯基-戊酸乙酯 Ethyl 2-phenyl-valerate | 0.13 | - | |
11,13-二甲基-12-十四烯-1-醇乙酸酯 11,13-dimethyl-12-tetradecene-1-ol acetate | 0.05 | - | |
1-甲基乙酸盐(酯) 1-methyl acetate (ester) | 0.08 | - | |
1,2-苯二甲酸,双(2-甲基丙基)酯 1,2-phthalic acid, bis (2-methylpropyl) ester | 0.08 | - | |
9-十八烯酸(2-苯基-1,3-二氧戊环-4-基)甲酯 9-octadecaenoic acid (2-phenyl-1,3-dioxopenyl-4-yl) methyl ester | - | 0.03 | |
壬酸乙酯Ethyl nonanoate | - | 0.05 | |
十四烷酸乙酯 Ethyl Myristate | - | 0.12 | |
邻苯二甲酸正丁酯 N-butyl phthalate | - | 0.12 | |
邻苯二甲酸二正辛酯 Di-n-octyl phthalate | - | 0.06 | |
1-丁醇,3-甲基乙酸酯 1-butanol, 3-methylacetate | - | 0.07 | |
醇类 Alcohols | 1-庚三醇 1-heptanol | 0.21 | 0.21 |
β-苯乙醇 β-phenylethanol | 21.81 | 19.73 | |
2,3-丁二醇 2,3- butane diol | 0.36 | - | |
3-甲基-2-己醇 3-methyl-2-hexanol | - | 0.09 | |
类别 Variety | 化合物 Compound | 相对百分含量Relative content (%) | |
处理前Before | 处理后After | ||
酮类 Ketones | 1-(2-羧基-4,4-二甲基环丁烯基)-1-丁烯-3-酮 1-(2-carboxyl-4,4-dimethylcyclobutanenol)-1-butene-3-one | 0.16 | 0.05 |
2,4,5,6,7,7a-六氢-3-(1-甲基乙基)-7a-甲基,1H-2-茚酮 2,4,5,6,7,7a-hexahydro-3-(1-methylethyl)-7a-methyl, 1h-2-indenone | 0.98 | 0.59 | |
4-(5,5-二甲基-1-氧螺环[2.5]辛-4-基)-3-丁烯-2-酮 4-(5,5-dimethyl-1-oxyspiro [2.5] oct-4-yl)-3-butene-2-one | 0.33 | - | |
1-(2,6,6-三甲基-1-环己烯-1-基)-1-戊烯-3-酮 1-(2,6,6-trimethyl-1-cyclohexene-1-yl)-1-pentene-3-one | 0.13 | - | |
1,8-二甲基-8,9-环氧-4-异丙基-螺环[4.5]癸-7-酮 1,8-dimethyl-8,9-epoxy-4-isopropyl-spiro [4.5] decyl-7-one | - | 0.13 | |
醛类 Aldehyde | 苯甲醛 Benzaldehyde | 1.84 | 1.87 |
2,5-二甲基苯甲醛 2,5-dimethylbenzaldehyde | 0.27 | 0.37 | |
3-(2,6,6-三甲基-1-环己烯-1-基)-2-丙烯醛 3-(2,6,6-trimethyl-1-cyclohexene-1-yl)-2-acrolein | 0.36 | 0.32 | |
2-[4-甲基-6-(2,6,6-三甲基环己-1-烯基)六-1,3,5-三烯基]环己-1-烯-1-甲醛 2-[4-methyl-6-(2,6,6-trimethylcyclohex-1-enyl) hexa-1,3,5-trienyl]cyclohex-1-ene-1-formaldehyde | 0.08 | 0.04 | |
烷类 Alkanes | 3-乙基-5-(2-乙基丁基)-十八烷 3-ethyl-5-(2-ethyl butyl)-octadecane | 0.38 | 0.79 |
二甲基-2-辛烷-环丁烷 Dimethyl-2-octane-cyclobutane | 0.67 | 0.40 | |
十七烷 Heptadecane | - | 0.18 | |
二十一烷 Decane | - | 0.19 | |
酚类 Phenols | 3,5-双(1,1-二甲基乙基)-苯酚 3,5-bis (1,1-dimethylethyl)-phenol | - | 0.16 |
含硫化合物 Sulfur compounds | 3-巯基-L-缬氨酸 3-mercapto-l-valine | 8.48 | 8.48 |
叔十六烷硫醇 Tertiary cetane mercaptan | - | 0.04 | |
其他类 Others | 十二烯基丁二酸酐 2-dodecenylsuccinic anhydride | 0.03 | 0.05 |
苄基-N-(1-苄基-2-羟乙基)-N-甲基氨基甲酸酯 Benzyl-n-(1-benzyl-2-hydroxyethyl)-N-methylcarbamate | 0.04 | - | |
2,5,8-三甲基-1,2-二氢萘 2,5,8-trimethyl-1,2-dihydronaphthalene | 0.07 | - | |
2-2-肉豆醇酰基,泛酰巯基乙胺 2-2-crotonoyl, pan acyl Mercaptoethylamine | - | 0.03 | |
1-甲基-3-(1-甲基乙基)-苯 1-methyl-3-(1-methylethyl)-benzene | - | 0.03 | |
4-苄氧基-6-羟基甲基-四氢吡喃-2,3,5-三醇 4-benzyloxy-6-hydroxymethyl-tetrahydropyran-2,3,5-triol | - | 0.05 | |
4-烯丙基-2-甲氧基苯基乙酸盐 4-allyl-2-methoxyphenyl acetate | - | 0.05 | |
1,2-二氢-2,5,8-三甲基萘 1,2-dihydro-2,5,8-trimethylnaphthalene | - | 0.07 | |
2,6-二十六酸,L-(+)-抗坏血酸 2,6-hexanoic acid, L-(+)-ascorbic acid | - | 0.08 | |
(1-羟基-4-氧代-1-苯基对羟基喹啉-3-基)氨基甲酸苄酯 N-Benzyln-(1-hydroxy-4-oxo-1-phenylp-hydroxyquinoline-3-yl) carbamate | - | 0.15 |
表5
超声处理前后模型酒中挥发性物质的变化"
种类 Type | 化合物 Compound | 相对百分含量Relative content (%) | |
---|---|---|---|
处理前 Before | 处理后After | ||
酯类 Esters | 己酸乙酯 Ethyl hexanoate | 1.26 | 0.83 |
丁酸-3-甲基丁酯 Butyrate-3-methyl-butyl | 4.45 | 3.26 | |
甲酸辛酯 Octyl formate | 1.79 | 0.93 | |
2-甲基丁酸戊酯 Amyl 2-methyl butyrate | 26.06 | 12.66 | |
3-戊酸-甲基丁酯 3-methyl-butyl valerate | 3.17 | 0.83 | |
1-甲基乙酸丁酯 1-Buty-methylacetate | 2.24 | 1.13 | |
3-甲基己基丁酸酯 3-methylhexylbutyrate | 1.32 | 0.99 | |
己酸异戊酯 Isopentyl hexanoate | 7.83 | 4.69 | |
己酸-2-甲基丁酯 2-methyl-butyl hexanoate | 0.93 | 0.60 | |
壬酸乙酯 Ethyl nonanoate | 1.02 | 0.76 | |
庚酸-3-甲基丁酯 3-methyl-butyl heptanate | 1.00 | 0.75 | |
辛酸-3-甲基丁酯 Octanoic acid-3-methyl butyl ester | 1.33 | 1.30 | |
丙二酸二乙酯 Diethyl malonate | 0.92 | 0.38 | |
2-甲基-3-甲基丙酸丁酯 2-methyl-3-methyl-butyl propionate | 0.78 | 0.61 | |
戊酸戊酯 Amyl valerate | - | 1.08 | |
辛酸乙酯 Ethyl caproate | - | 2.57 | |
十五烷酸-3-甲基丁酯 Pentadecanoic acid-3-methyl butyl ester | - | 4.40 | |
月桂酸异戊酯 Isoamyl Laurate | - | 12.57 | |
十六酸乙酯 Ethyl palmitate | - | 1.58 | |
3-甲基丁酸丁酯 3-methyl-butyl butyrate | - | 0.37 | |
辛酸乙酯 Ethyl caproate | - | 1.74 | |
癸酸乙酯 Ethyl decanoate | - | 0.37 | |
己酸-2-乙氧基乙酯 2-ethoxyethyl hexanoate | - | 1.01 | |
壬酸-3-甲基丁酯 3-methyl-n-butyl nonanoate | - | 0.88 | |
甲酸-2-甲基丁酯 Formic acid-2-methyl butyl ester | - | 1.22 | |
醛类 Aldehyde | 3-甲基丁醛 3-Methylbutyraldehyde | 0.70 | 0.83 |
苯甲醛 Benzaldehyde | - | 0.71 | |
2,4-二甲基苯甲醛 2,4-dimethylbenzaldehyde | 3.08 | - | |
醇类 Alcohols | 苯乙醇 Phenylethanol | 0.75 | 1.01 |
1-壬醇 1-Nonanol | 2.87 | 4.30 | |
1-癸醇 1-Decanol | 1.35 | 1.61 | |
3-甲基-苯甲酸-丁醇 3-Methyl-benzoic acid-butanol | 15.92 | 17.25 | |
5-甲基-2-(1-甲基乙基)-1-己醇 5-methyl-2-(1-methylethyl)-1-hexanol | - | 1.07 | |
3-甲基-甲酸-丁醇 3-methyl-formic acid-butanol | 6.28 | - | |
3-乙酸-甲基-1-丁醇 3-Acetic acid-methyl-1-butanol | 1.82 | - | |
2-丁基-辛醇 2-butyl-octanol | 0.65 | - | |
2,2,4,4-四甲基-3-(四氢呋喃基) 3-戊醇 2,2,4,4-tetramethyl-3-(tetrahydrofuran group) 3-pentanol | 1.58 | - | |
烷类 Alkanes | 戊烷 Pentane | 2.54 | 4.20 |
十二甲基-环己烷 Dodecyl cyclohexane | 1.06 | 2.12 | |
十四甲基-环庚烷 Tetramethyl cycloheptane | 2.15 | 3.21 | |
十四烷 Tetradecane | 1.04 | - | |
十六烷 Cetane | 0.84 | - | |
十七烷 Heptadecane | 0.54 | - | |
苯类 Benzene | 1,2,4-三甲基-苯 1,2,4-trimethyl-benzene | 1.69 | 2.49 |
1,2,3,5-四甲基-苯 1,2,3,5-tetramethyl-benzene | 0.39 | - | |
酚类 Phenols | 2,4-二(1,1-二甲基乙基)-苯酚 2,4-bis (1,1-dimethylethyl)-phenol | - | 3.46 |
其他类 Others | 萘 Naphthalene | 0.42 | - |
2-丁基-萘 2-butyl-naphthalene | 0.47 | - |
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