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Development of a texture evaluation system for winter jujube (Ziziphus jujuba ‘Dongzao’)
KONG Xia-bing, XU Min, WAN Hao-liang, HAN Ling-xi, LIU Xiao-li, LI Qing-jun, HAO Bian-qing, ZHANG Shao-jun, LI Xiao-ming, LIU Yi-hui, NIE Ji-yun
2022, 21 (12): 3658-3668.   DOI: 10.1016/j.jia.2022.09.007
Abstract262)      PDF in ScienceDirect      

Winter jujube (Ziziphus jujuba ‘Dongzao’) is an excellent late maturing variety of fresh-eating jujube in China.  Fruit texture is an important indicator of sensory quality.  To investigate the correlations among texture indices and establish an evaluation system for winter jujube texture, we used the TMS-Touch instrument to perform a texture profile analysis (TPA) on 1 150 winter jujubes from three major producing areas in China.  Eight indices and their best-fit distribution were obtained, including fracture (Pearson), hardness (InvGauss), adhesive force (Weibull), adhesiveness (LogLogistic), cohesiveness (LogLogistic), springiness (BetaGeneral), gumminess (InvGauss), and chewiness (InvGauss).  Based on the best-fit distribution curves, each index was divided into five grades (lower, low, medium, high and higher) by the 10th, 30th, 70th and 90th percentiles.  Among the texture indices, 82% of the correlation coefficients were highly significant (P<0.01); meanwhile, chewiness was significantly (P<0.01) and positively correlated with springiness and gumminess, of which the correlation coefficients were up to 0.8692 and 0.8096, respectively.  However, adhesiveness was significantly (P<0.01) and negatively related to adhesive force with a correlation coefficient of –0.7569.  Among hardness, cohesiveness, springiness, gumminess, and chewiness, each index could be well fitted by a multiple linear regression with the remaining four indices, with the coefficients above 0.94 and the mean fitting error and mean prediction error lower than 10%.  A comprehensive evaluation model was consequently established based on factor analysis to evaluate the texture quality of winter jujube.  The results demonstrated that winter jujube with higher comprehensive scores generally exhibited higher springiness and chewiness, but had lower adhesive force and adhesiveness.  We used factor analysis and clustering analysis to divide the eight studied texture into four groups (cohesive factor, adhesive-soft factor, tough-hard factor, and crispness factor), whose representative indices were springiness, adhesiveness, hardness, and fracture, respectively.  Overall, this study investigated the variation in each index of winter jujube texture, explored the association among these indices, screened the representative indices, and established a texture evaluation system.  The results provide a methodological basis and technical support for evaluating winter jujube texture.

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Evaluation of sugar and organic acid composition and their levels in highbush blueberries from two regions of China
ZHANG Jia, NIE Ji-yun, LI Jing, ZHANG Hui, LI Ye, Saqib FAROOQ, Syed Asim Shah BACHA, WANG Jie
2020, 19 (9): 2352-2361.   DOI: 10.1016/S2095-3119(20)63236-1
Abstract117)      PDF in ScienceDirect      
Sweet and sour are the most important taste of blueberries, and they are produced by sugar and acid, respectively.  Their contributions to the taste depend not only on the levels of sugar and acid, but also on the types and relative proportions of sugar and acid.  Therefore, it is very important to evaluate the composition and levels of sugar and acid in blueberries.  Regional differences and variety diversity also affect the sugar and acid characteristics of fruits.  Therefore, this study selected two main producing regions in northern China (Weihai and Yingkou) to examine the sugar and acid characteristics of 11 common blueberry cultivars.  The indexes measured included soluble sugars, organic acids, soluble solid content and titratable acidity.  The results showed that glucose and fructose were the major sugars, and citric acid and quinic acid were the major organic acids.  Correlation analysis showed that glucose, fructose, and sucrose were positively correlated with total sugar content; the citric acid content was positively correlated with the titratable acidity and total organic acids.  Titratable acidity, glucose, fructose, sucrose, total sugar content, citric acid, shikimic acid and total acid content of the blueberries varied significantly between regions (P<0.05).  In general, compared with Weihai blueberries, Yingkou blueberries had higher sugar content and lower acid content.  The results of this study may provide useful references for the evaluation of sweet and sour flavors and cultivar selection of blueberries.
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Multi-mycotoxin exposure and risk assessments for Chinese consumption of nuts and dried fruits
WANG Yu-jiao, NIE Ji-yun, YAN Zhen, LI Zhi-xia, CHENG Yang, Saqib Farooq
2018, 17 (07): 1676-1690.   DOI: 10.1016/S2095-3119(18)61966-5
Abstract475)      PDF in ScienceDirect      
In this study, 15 mycotoxins were detected in 233 nut and dried fruit samples from China.  The 15 mycotoxins included aflatoxins (AFs: AFB1, AFB2, AFG1 and AFG2), trichothecene toxins (TCs: T-2, ZEA, ENA, ENA1, ENB, ENB1 and BEA), Alternaria toxins (ATs: TEN, AOH and AME) and ochratoxin A (OTA).  The mycotoxins were detected in 47.6% of the samples and all 15 of the mycotoxins were found.  Two samples were positive for AFB1 and exceeded the maximum tolerable levels allowed in China.  The contamination levels of the mycotoxins found in nuts, dried jujubes, raisins, dried figs and dried longans were in the ranges of 0.1–462.7, 0.2–247.3, 0.8–10.1, 0.2–384.1 and 0.1–89.2 μg kg–1, respectively.  Dried figs (80.0%) had the highest incidence of mycotoxins, followed by dried longans (60.0%), dried jujubes (57.1%), nuts (43.6%) and raisins (26.7%).  The estimated daily intake (EDI) values of each individual mycotoxin and all of the mycotoxins collectively were calculated by both the deterministic approach (DA) and the probability approach (PA).  For risk characterization, dietary exposure to TCs, ATs and OTA through consumption of nuts and dried fruits according to both approaches, showed no health risk to Chinese adults by exposure to either individual mycotoxins or in combination.  To the best of our knowledge, this is the first work in which risk assessment of multimycotoxins is performed, specifically including the emerging ENNs and BEA, in nuts and dried fruits of China. 
 
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Evaluation indices of sour flavor for apple fruit and grading standards
YAN Zhen, ZHENG Li-jing, NIE Ji-yun, LI Zhi-xia, CHENG Yang
2018, 17 (05): 994-1002.   DOI: 10.1016/S2095-3119(17)61795-7
Abstract495)      PDF in ScienceDirect      
In order to establish grading standards of evaluation indices for sour flavor of apples, 10 indices of samples from 106 apple cultivars were tested, including: malic acid (Mal), oxalic acid (Oxa), citric acid (Cit), lactic acid (Lac), succinic acid (Suc), fumaric acid (Fum), total organic acids (ToA, the sum of the six organic acids tested), titratable acid (TiA), acidity value (AcV), and pH value.  For most of the cultivars studied (85.8%), the order of the organic acid contents in apples was Mal>Oxa>Cit>Lac>Suc>Fum.  Mal was the dominant organic acid, on average, accounting for 94.5% of ToA.  Among the 10 indices, the dispersion of pH value was the smallest with a coefficient of variation of only 8.2%, while the coefficients of variation of the other nine indices were larger, ranging between 31 and 66%.  There were significant linear relationships between Mal and two indices (ToA and AcV) as well as between ToA and AcV.  There were significant logarithmic relationships between pH value and four indices: Mal, TiA, ToA, and AcV.  All the equations had very high fitting accuracy and can be used to accurately predict related indices.  According to this study, Mal, ToA, and AcV of apple were normally distributed, TiA was close to normally distributed, whereas pH value had a skewed distribution.  Using the fitted normal distribution curves, the grading standards of Mal, TiA, ToA, and AcV were established.  The grading node values of pH value were obtained using the logarithmic relationship between pH value and Mal.  The grading standards of these five indices can be used to evaluate the sour flavor of apple.  This study provides a scientific basis for evaluating apple flavor and selecting apple cultivars.
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Assessing the concentration and potential health risk of heavy metals in China’s main deciduous fruits
NIE Ji-yun, KUANG Li-xue, LI Zhi-xia, XU Wei-hua, WANG Cheng, CHEN Qiu-sheng, LI An, ZHAO Xu-bo, XIE Han-zhong, ZHAO Duo-yong, WU Yong-long, CHENG Yang
2016, 15 (7): 1645-1655.   DOI: 10.1016/S2095-3119(16)61342-4
Abstract1754)      PDF in ScienceDirect      
To assess levels of contamination and human health risk, we analyzed the concentrations of the heavy metals lead (Pb), cadmium (Cd), chromium (Cr), and nickel (Ni) in China’s main deciduous fruits - apple, pear, peach, grape, and jujube. The concentration order of the heavy metals was Ni>Cr>Pb>Cd. In 97.5% of the samples, heavy metal concentrations were within the maximum permissible limits. Among the fruits studied, the heavy metal concentrations in jujube and peach proved to be the highest, and those in grape proved to be the lowest. Only 2.2% of the samples were polluted by Ni, only 0.4% of the samples were polluted by Pb, and no samples were polluted by Cd or Cr. Compared with the other fruits, the combined heavy metal pollution was significantly higher (P<0.05) in peach and significantly lower (P<0.05) in grape. For the combined heavy metal pollution, 96.9% of the samples were at safe level, 2.32% at warning level, 0.65% at light level, and 0.13% at moderate level. In the fruits studied, the contribution of heavy metals to the daily intake rates (DIR) followed the order of Ni>Cr>Pb>Cd. The highest DIR came from apple, while the lowest DIR came from grape. For each of the heavy metals, the total DIR from five studied fruits corresponded to no more than 1.1% of the tolerable daily intake, indicating that no significant adverse health effects are expected from the heavy metals and the fruits studied. The target hazard quotients and the total target hazard quotients demonstrated that none of the analyzed heavy metals may pose risk to consumers through the fruits studied. The highest risk was posed by apple, followed in decreasing order by peach and pear, jujube, and grape. We suggest that the main deciduous fruits (apple, pear, peach, grape, and jujube) of China’s main producing areas are safe to eat.
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Risk assessment and ranking of pesticide residues in Chinese pears
LI Zhi-xia, NIE Ji-yun, YAN Zhen, XU Guo-feng, LI Hai-fei, KUANG Li-xue, PAN Li-gang, XIE Han-zhong, WANG Cheng, LIU Chuan-de, ZHAO Xu-bo, GUO Yong-ze
2015, 14 (11): 2328-2339.   DOI: 10.1016/S2095-3119(15)61124-8
Abstract2376)      PDF in ScienceDirect      
The presence of pesticide residues in pears is a serious health concern. This study presents the results from a 2-year investigation (2013–2014) that used gas chromatography, GS/MS and UPLC/MS-MS to measure the levels of 104 pesticides in 310 pear samples. In 93.2% of the samples, 43 pesticides were detected, of which the maximum residue levels (MRLs) were exceeded in 2.6% of the samples. Multiple residues (two to eight compounds) were present in 69.7% of the samples; one sample contained nine pesticides and one sample contained 10. Only 6.8% of the samples did not contain residues. To assess the health risks, the pesticide residue data have been combined with daily pear consumption data for children and adult populations. A deterministic model was used to assess the chronic and acute exposures based on the Joint Meeting on Pesticide Residues (JMPR) method. A potential acute risk was demonstrated for children in the case of bifenthrin, which was found to be present at 105.36% of the acute reference dose (ARfD) value. The longterm exposure of the Chinese consumer to pesticide residues through the consumption of raw pears was far below the acceptable daily intake (ADI) criterion. Additionally, the matrix ranking scheme was used to classify risk subgroups of pesticides and pear samples. In general, 95.5% of samples were deemed to be safe and nine pesticides were classified as being of a relatively high risk. The findings indicated that the occurrence of pesticide residues in pears should not be considered a serious public health problem. Nevertheless, a more detailed study is required for vulnerable consumer groups, especially children. Continuous monitoring of pesticides in pears and tighter regulation of pesticide residue standards are recommended.
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