中国农业科学 ›› 2011, Vol. 44 ›› Issue (12): 2469-2475 .doi: 10.3864/j.issn.0578-1752.2011.12.008

• 植物保护 • 上一篇    下一篇

采用三角坐标图法快速筛选5%己唑醇悬浮剂配方

张大侠;刘 峰;张贵森;陈 波;杨晓楠
  

  1. 山东农业大学植物保护学院
  • 收稿日期:2010-12-13 修回日期:2011-03-20 出版日期:2011-06-15 发布日期:2011-06-15
  • 通讯作者: 刘峰

Rapid Screen Formulation for 5% Hexaconazole Suspension Concentrate Using Triangle-coordinate Figure

ZHANG Da-xia; LIU Feng; ZHANG Gui-sen; CHEN-Bo; YANG Xiao-nan
  

  1. 山东农业大学植物保护学院
  • Received:2010-12-13 Revised:2011-03-20 Online:2011-06-15 Published:2011-06-15

摘要:

【目的】建立快速筛选己唑醇悬浮剂最佳配方的实用方法。【方法】以5%己唑醇悬浮剂配方为例,将悬浮剂体系分为润湿分散体系和抗沉降体系,分别运用于三角坐标图法。将确定的3个供筛因素,作为三角坐标系的3个顶点,并研磨3个母液,再按照配方利用10 000转/min剪切条件进行调配制得配方,选用重要且快速简单的性能评价指标如粘度、贮存析水率、悬浮率和分散性等,在得到质量较优的配方区域的基础上,进一步筛选得到最优配方。【结果】得到了5%己唑醇悬浮剂理想的配方:5%己唑醇,0.5%NP-10,1%1602,3.5%木质素磺酸钠,0.025%黄原胶,2%硅酸镁铝,2.5%钠基膨润土,3%乙二醇,水补至100%。筛选过程中共需要约1 040 g样品,研磨和调制配方共耗时约13 h,比全部采用砂磨工艺可节省时间3/4,节省原材料1/2以上。【结论】三角坐标图法操作简便、节省材料,提高了悬浮剂配方筛选的科学性和效率,具有良好的实用性。

Abstract:

【Objective】The objective of this study is to build a rapid screening recipe of hexaconazole suspension concentrate. 【Method】The suspension system was divided into wetting dispersants and antisettling agents by using the method, and then used, respectively, to the triangle-coordinate figure. In order to shorten the screening period, the method replaced grinding with shearing to obtain samples, and the important and quality performance indices such as viscosity, water separation ratio, suspensibility and dispersion were selected. The optimum recipe was obtained by further screening, based on determining a better region in the triangle rectangular coordinate.【Result】The optimum formulation of 5% hexaconazole SC was determined: 5% hexaconazole, 0.5% NP-10, 1% 1602,3.5% VSI-B88, 0.025% XG, 2% magnesium aluminum silicatenf, 2.5% Na-Ben, 3% ethylene glycol and fill water to 100%. Throughout the selection process, 1 040 g sample and 13 hours were consumed, which was more efficient than the conventional method. That replaced grinding with shearing could save time 3/4 and save 1/2 or more raw materials.【Conclusion】The technological assay established in this study is a rapid, high efficient and simple tool for screening the formulation of SC.